(叔丁氧基羰基甲基)氯化三苯基磷合成路线 (共 11 条)
反应条件
1: (2-(tert-butoxy)-2-oxoethyl)triphenylphosphonium chloride With potassium hexamethylsilazane in tetrahydrofuran
T=-78°C; Inert atmosphere;
2: benzaldehyde in tetrahydrofuran
T=-78 - 20°C; Wittig reaction; Inert atmosphere; optical yield given as percent de;
参考文献
Byrne, Peter A.; Rajendran, Kamalraj V.; Muldoon, Jimmy; Gilheany, Declan G.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 17 p. 3531 - 3537