反应条件
in hexane
soln. of educts was refluxed for 32 h; mixt. was filtd., washed with hexane, solvent was evaporated under reduced pressure, vac. distn., product distd. at 158-162° (1 Torr), elem. anal.;
参考文献
Bai, J.; Niedenzu, K.; Serwatowska, J.; Serwatowski, J.
Inorganic Chemistry, 1992 , vol. 31, p. 228 - 233
