吡嗪-2,6-二羧酸二甲酯合成路线 （共 4 条）
反应条件
2-azidoethanol; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) T=120°C; P=29420.3 Torr; 16 h;
参考文献
Takeuchi; Suzuki; Sato
Synthesis, 1990 , vol. 1, # 10 p. 923 - 924
反应条件
1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h 1.2: 20 h / |Reflux 2.1: lithium carbonate / 0.5 h 2.2: 3 h / 0 °C View Scheme
参考文献
Nikishkin, Nicolai I.; Huskens, Jurriaan; Ansari, Seraj A.; Mohapatra, Prasanta K.; Verboom, Willem
New Journal of Chemistry, 2013 , vol. 37, # 2 p. 391 - 402
反应条件
1: With lithium carbonate 0.5 h; 2: With MMPP T=0°C; 3 h;
参考文献
Nikishkin, Nicolai I.; Huskens, Jurriaan; Ansari, Seraj A.; Mohapatra, Prasanta K.; Verboom, Willem
New Journal of Chemistry, 2013 , vol. 37, # 2 p. 391 - 402
反应条件
1: With sodium hydroxide in tetrahydrofuran; water
1 h;
2: With hydrogenchloride in tetrahydrofuran; water
参考文献
Nikishkin, Nicolai I.; Huskens, Jurriaan; Ansari, Seraj A.; Mohapatra, Prasanta K.; Verboom, Willem
New Journal of Chemistry, 2013 , vol. 37, # 2 p. 391 - 402
