1.1: 2.58 g / H2 / Pd/C / ethyl acetate / 20 h 2.1: trimethylsilyl chloride / diethyl ether / 1 h / 20 °C 2.2: 62 percent / tert-butylmagnesium chloride / diethyl ether / 3 h / 20 °C View Scheme
参考文献
Beusker, Patrick H.; Veldhuis, Harald; Van Den Bossche, Bianca A. C.; Scheeren, Hans W.
European Journal of Organic Chemistry, 2001 , # 9 p. 1761 - 1768
1.1: 2.58 g / H2 / Pd/C / ethyl acetate / 20 h 2.1: trimethylsilyl chloride / diethyl ether / 1 h / 20 °C 2.2: 62 percent / tert-butylmagnesium chloride / diethyl ether / 3 h / 20 °C 3.1: 87 percent / triethylamine; 4-(dimethylamino)pyridine / CH2Cl2 / 20 h / 20 °C View Scheme
参考文献
Beusker, Patrick H.; Veldhuis, Harald; Van Den Bossche, Bianca A. C.; Scheeren, Hans W.
European Journal of Organic Chemistry, 2001 , # 9 p. 1761 - 1768
