3-chloro-benzenecarboperoxoic acid in methanol Ambient temperature;

dihydrogen peroxide; iron powder in ethanol Fenton Reaction;

dihydrogen peroxide; iron(III) cation; Reduced nicotinamide-adenine dinucleotide in ethanol Fenton Reaction; Reagent/catalyst;

dihydrogen peroxide; iron(III) cation; Reduced nicotinamide-adenine dinucleotide in ethanol Fenton Reaction; Reagent/catalyst;

dihydrogen peroxide; iron(III) cation; Reduced nicotinamide-adenine dinucleotide in ethanol Fenton Reaction; Reagent/catalyst;

1: 85 percent / NaClO4 / N,N-dimethyl-acetamide 2: 70 percent / Amberlite IRA-402 (HCO3-), H2O / 192 h / 3 - 4 °C 3: 69 percent / K2CO3 / dimethylformamide / Ambient temperature 4: H2 / Raney Ni / H2O / 1.5 h / 760 Torr / Ambient temperature 5: Et3N / methanol / 72 h / -18 °C 6: aq. acid / 25 °C / pH 3.34, var. pH, temp. View Scheme

1: 3.37 g / N,N-dimethyl-acetamide / 6.5 h / 13 - 14 °C 2: Amberlite IRA-402 (HCO3-) / H2O 3: aq. NaOH / 0.25 h / Heating 4: H2; 1N aq. HCl / Raney Ni W-2 / H2O / 4.5 h / 760 Torr / Ambient temperature 5: Amberlite IRA-402 (OH-) / H2O View Scheme

1: 85 percent / NaClO4 / N,N-dimethyl-acetamide 2: 70 percent / Amberlite IRA-402 (HCO3-), H2O / 192 h / 3 - 4 °C 3: 69 percent / K2CO3 / dimethylformamide / Ambient temperature 4: 61 percent / 0.1 N aq. HCl / 3.5 h / Ambient temperature 5: HCl / ethanol View Scheme