4-(4-氯苯基)-2-丁酮合成路线 （共 19 条）
反应条件
wet cells of Candida parapsilosis ATCC 7330 in aq. phosphate buffer; acetone T=25°C; pH=6.5; 7 h; Microbiological reaction; enantioselective reaction;
参考文献
RSC Advances, , vol. 4, # 5 p. 2257 - 2262
反应条件
palladium diacetate; silver(I) acetate; antimony trichloride; acetic acid T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-Ichi; Ohe, Kouichi; Uemura, Sakae
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 8 p. 2341 - 2348
反应条件
titanium(III) chloride in acetic acid T=5°C; other α,β-unsaturated carbonyl compounds, regioselectivity of aryl radical addition; Product distributionRate constantMechanism;
参考文献
Citterio, Attilio; Minisci, Francesco; Vismara, Elena
Journal of Organic Chemistry, 1982 , vol. 47, # 1 p. 81 - 88
反应条件
hydrogenchloride; TiCl3; sodium nitrite 1.) 0-5 degC, 2.) Acetone, 30 min, 40 degC;
参考文献
Citterio, Attilio; Vismara, Elena
Synthesis, 1980 , # 4 p. 291 - 292
参考文献
Journal of the American Chemical Society, , vol. 86, p. 1649 - 1650
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; sodium formate; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide in water T=60°C; 7 h; Inert atmosphere; chemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 75, # 9 p. 2981 - 2988
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine T=80°C; P=15001.5 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
New Journal of Chemistry, , vol. 33, # 5 p. 969 - 971
反应条件
1: sodium hydroxide / water / 0 - 20 °C 2: palladium 10 on activated carbon; hydrogen / methanol / 3 h / 1551.49 Torr View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 12 p. 3784 - 3787
反应条件
titanium(III) chloride in acetic acid T=5°C; 2 h; var. conc. of reagents; Product distributionRate constant;
参考文献
Journal of Organic Chemistry, , vol. 47, # 1 p. 81 - 88
