4-萘-1-基丁烷-2-酮合成路线 （共 28 条）
反应条件
1: in tetrahydrofuran T=5 - 20°C; 2 h; 2: With water; ammonium chloride in tetrahydrofuran
参考文献
JANSSEN PHARMACEUTICA N.V.
Patent: WO2007/436 A1, 2007 ;
Location in patent: Page/Page column 37 ;
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=80°C; 1.5 h;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3558 - 3563
反应条件
RuCl3H(p-cymene)2; immobilized lipase from Pseudomonas cepacia; triethylamine in dichloromethane T=20 - 25°C; Acetylation; oxidation; reduction; 48 h; Enzymatic reaction;
参考文献
Lee; Huh; Kim; Jung; Koh; Park
Organic letters, 2000 , vol. 2, # 15 p. 2377 - 2379
反应条件
silver(I) acetate; palladium diacetate in acetic acid T=25°C; 24 h;
参考文献
Cho, Chan Sik; Tanabe, Koichiro; Uemura, Sakae
Tetrahedron Letters, 1994 , vol. 35, # 8 p. 1275 - 1278
反应条件
Ni-2,2'-dipyridylamine in ethanol T=20°C; Arylation; Electrolysis;
参考文献
Courtois, Valerie; Barhdadi, Rachid; Condon, Sylvie; Troupel, Michel
Tetrahedron Letters, 1999 , vol. 40, # 33 p. 5993 - 5996
反应条件
C48H42Cl2O4P4Pd2; sodium acetate in N,N-dimethyl-formamide T=90°C; Heck reaction; 6 h; regioselective reaction;
参考文献
Sauza, Alejandro; Morales-Serna, Jose Antonio; Garcia-Molina, Monica; Gavino, Ruben; Cardenas, Jorge
Synthesis, 2012 , vol. 2012, # 2 p. 272 - 282
反应条件
palladium diacetate; silver(I) acetate; antimony trichloride; acetic acid T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-Ichi; Ohe, Kouichi; Uemura, Sakae
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 8 p. 2341 - 2348
反应条件
palladium on activated charcoal
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
反应条件
1: LiAlH4; diethyl ether 2: SOCl2; pyridine; toluene 3: ethanol / Erwaermen des Reaktionsprodukts mit wss. NaOH 4: palladium/charcoal View Scheme
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
反应条件
1: ethanol / Erwaermen des Reaktionsprodukts mit wss. NaOH 2: palladium/charcoal View Scheme
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
