4-萘-1-基丁烷-2-酮合成路线 （共 28 条）
反应条件
1: SOCl2; pyridine; toluene 2: ethanol / Erwaermen des Reaktionsprodukts mit wss. NaOH 3: palladium/charcoal View Scheme
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
反应条件
potassium carbonate in ethanol
参考文献
Boatman,S. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 3321 - 3324
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; sodium formate; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide in water T=60°C; 5 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Xuefeng; Li, Liangchun; Tang, Yuanfu; Zhong, Ling; Cun, Linfeng; Zhu, Jin; Liao, Jian; Deng, Jingen
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 2981 - 2988
反应条件
RhCl(cycloocta-1,5-diene){3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazol-2-ylidene}; sodium hydroxide; cyclooctadiene in toluene T=60°C; 6 h; Catalytic behavior;
参考文献
Penafiel, Itziar; Pastor, Isidro M.; Yus, Miguel; Esteruelas, Miguel A.; Olivan, Montserrat
Organometallics, 2012 , vol. 31, # 17 p. 6154 - 6161
反应条件
(i), (ii) aq. NaOH; Multistep reaction;
参考文献
Zimmerman, Howard E.; Blinn, James R.
Tetrahedron, 1981 , vol. 37, # 19 p. 3237 - 3244
反应条件
sodium hydroxide in water 4 h; Heating;
参考文献
Aulenta, Francesca; Berndt, Mathias; Bruedgam, Irene; Hartl, Hans; Soergel, Sebastian; Reissig, Hans-Ulrich
Chemistry - A European Journal, 2007 , vol. 13, # 21 p. 6047 - 6062
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran / 0.33 h / 0 °C 1.2: tetrahydrofuran / 0.33 h / 0 °C 2.1: sodium hydroxide / H2O / 10 h / 20 °C 2.2: 1.69 g / H2O / 4 h / Heating View Scheme
参考文献
Aulenta, Francesca; Berndt, Mathias; Bruedgam, Irene; Hartl, Hans; Soergel, Sebastian; Reissig, Hans-Ulrich
Chemistry - A European Journal, 2007 , vol. 13, # 21 p. 6047 - 6062
反应条件
Pt/Al2O3; colloid; acetic acid Hydrogenation;
参考文献
Gibson et al.
Journal of the Chemical Society, 1926 , p. 2253
参考文献
Tatta,K.R.; Bardhan,J.C.
Journal of the Chemical Society [Section] C: Organic, 1968 , vol. <C>, p. 893 - 900
反应条件
1: phosphorus pentachloride; tetrachloroethane / 140 - 150 °C / Eintragen des Reaktionsprodukts in eine mit Chlorwasserstoff gesaettigte aetherische Loesung von Zinn(II)-chlorid und Destillieren mit Wasserdampf 2: diluted NaOH-solution 3: colloid/al platinum; glacial acetic acid / Hydrogenation View Scheme
参考文献
Gibson et al.
Journal of the Chemical Society, 1926 , p. 2253
