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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
35066-22-9
合成路线
（共 11 条）
35066-22-9
→
反应条件
5978-70-1
(R)-(-)-2-辛醇
反应条件
1: dimethylformamide; hexamethylphosphoric acid triamide / 16 h / 55 °C 2: 100 percent / LiAlH4 / tetrahydrofuran 3: 56 percent / pyridine 4: 95 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Iriye, Ryozo; Takai, Katsuki; Noguchi, Masakazu
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 2 p. 199 - 202
35066-22-9
→
反应条件
124-13-0
正辛醛
反应条件
DMBI in tetrahydrofuran 5 h; Heating;
参考文献
Chikashita, Hidenori; Ide, Hisao; Itoh, Kazuyoshi
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5400 - 5405
35066-22-9
→
反应条件
3025-30-7
2,4-癸二烯酸乙酯
反应条件
1: 58 percent / tetrabutylammonium bromide (TBAB) / benzene; H2O / 40 h / Heating 2: 52 percent / benzene / 14 h / Heating 3: Pd(Ph3P)4 / tetrahydrofuran / 6 h View Scheme
参考文献
Sakai, Takashi; Seko, Katsuhiko; Tsuji, Akihiro; Utaka, Masanori; Takeda, Akira
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 1101 - 1106
35066-22-9
→
反应条件
6169-06-8
(S)-(+)-2-辛醇
反应条件
1: 35 percent / dimethylformamide; hexamethylphosphoric acid triamide / 1 h / 55 °C 2: 100 percent / LiAlH4 / tetrahydrofuran 3: 56 percent / pyridine 4: 93 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Iriye, Ryozo; Takai, Katsuki; Noguchi, Masakazu
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 2 p. 199 - 202
35066-22-9
→
反应条件
1117-86-8
1,2-辛二醇
反应条件
1: dimethylformamide; hexamethylphosphoric acid triamide / 16 h / 55 °C 2: 100 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Iriye, Ryozo; Takai, Katsuki; Noguchi, Masakazu
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 2 p. 199 - 202
35066-22-9
→
反应条件
2548-87-0
反-2-辛烯醛
反应条件
1: Ionicliquid [bmim]HSO4 / 0.08 h / |Microwave irradiation 2: sodium ethanolate / dimethyl sulfoxide / 16 h / 120 °C 3: water / 0.13 h / |Microwave irradiation View Scheme
参考文献
Gupta, Neeraj; Kaur, Manvinder; Shallu; Gupta, Neeru; Kad, Goverdhan Lal; Singh, Jasvinder
Natural Product Research, 2013 , vol. 27, # 6 p. 548 - 553
64-17-5
乙醇
+
35066-22-9
→
反应条件
33861-21-1
反应条件
Ionicliquid [bmim]HSO4 0.0833333 h; Microwave irradiation;
参考文献
Gupta, Neeraj; Kaur, Manvinder; Shallu; Gupta, Neeru; Kad, Goverdhan Lal; Singh, Jasvinder
Natural Product Research, 2013 , vol. 27, # 6 p. 548 - 553
35066-22-9
→
反应条件
18836-52-7
反应条件
1: 58 percent / tetrabutylammonium bromide (TBAB) / benzene; H2O / 40 h / Heating 2: 1.) 2.1 N methanolic NaOMe / 1.) methanol, room temp., 5 min, 2.) reflux, 2 h 3: 70 percent / (Ph3P)4Pd / tetrahydrofuran / 6 h / Heating View Scheme
参考文献
Sakai, Takashi; Seko, Katsuhiko; Tsuji, Akihiro; Utaka, Masanori; Takeda, Akira
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 1101 - 1106
35066-22-9
→
反应条件
1117-86-8
1,2-辛二醇
反应条件
1: dimethylformamide; hexamethylphosphoric acid triamide / 16 h / 55 °C 2: 100 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Iriye, Ryozo; Takai, Katsuki; Noguchi, Masakazu
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 2 p. 199 - 202
35066-22-9
→
反应条件
42134-50-9
反应条件
1: Ionicliquid [bmim]HSO4 / 0.08 h / |Microwave irradiation 2: sodium ethanolate / dimethyl sulfoxide / 16 h / 120 °C 3: water / 0.13 h / |Microwave irradiation 4: dihydrogen peroxide; sodium hydroxide / water / 2 h / pH 8 - 8.5 View Scheme
参考文献
Gupta, Neeraj; Kaur, Manvinder; Shallu; Gupta, Neeru; Kad, Goverdhan Lal; Singh, Jasvinder
Natural Product Research, 2013 , vol. 27, # 6 p. 548 - 553
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