3-(二甲基氨基)-1-(3-甲氧基苯基)-1-丙酮合成路线 (共 4 条)
反应条件
1: in acetonitrile T=3 - 25°C; Mannich Reaction; 2: With sodium hydroxide in water Mannich Reaction;
参考文献
Gruenenthal GmbH
Patent: US2009/253936 A1, 2009 ;
Location in patent: Page/Page column 9 ;
反应条件
hydrogenchloride in ethanol 2 h; Heating; Yield given;
参考文献
Dorsch, Dieter; Schadt, Oliver; Blaukat, Andree
Patent: US2008/249095 A1, 2008 ;
Location in patent: Page/Page column 46 ;
反应条件
hydrogenchloride; formaldehyd
参考文献
Knott
Journal of the Chemical Society, 1947 , p. 1196,1200
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=20°C; Product distribution / selectivity;
参考文献
Gruenenthal GmbH
Patent: US2009/253936 A1, 2009 ;
Location in patent: Page/Page column 10 ;