Alpha-正丁基苯乙腈合成路线 （共 19 条）
反应条件
sodium amide in toluene; benzene T=80°C; 1 h;
参考文献
Hartmann, Rolf W.; Batzl, Christine
Journal of Medicinal Chemistry, 1986 , vol. 29, # 8 p. 1362 - 1369
反应条件
ruthenium-grafted hydrotalcite T=180°C; 20 h;
参考文献
Motokura, Ken; Nishimura, Daisuke; Mori, Kohsuke; Mizugaki, Tomoo; Ebitani, Kohki; Kaneda, Kiyotomi
Journal of the American Chemical Society, 2004 , vol. 126, # 18 p. 5662 - 5663
反应条件
sodium hydroxide; tetrabutylammomium bromide in water
参考文献
Rohm and Haas Company
Patent: US4225723 A1, 1980 ;
反应条件
sodium hydroxide 28 h; Ambient temperature;
参考文献
Fujihara, Hisashi; Imaoka, Koji; Furukawa, Naomichi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 333 - 336
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,3,5-trimethyl-benzene T=20 - 140°C; 10.1667 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Shang, Rui; Ji, Dong-Sheng; Chu, Ling; Fu, Yao; Liu, Lei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 19 p. 4470 - 4474
反应条件
1: n-capronitrile With n-butyllithium in tetrahydrofuran T=-78°C; 0.25 h; 2: Phenyl[2-(trimethylsilyl)phenyl]iodonium trifluoromethanesulfonate With tetrabutyl ammonium fluoride in tetrahydrofuran T=0 - 20°C; 0.916667 h;
参考文献
Kamila, Sukanta; Koh, Benjamin; Biehl, Edward R.
Synthetic Communications, 2006 , vol. 36, # 23 p. 3493 - 3507
反应条件
diethyl ether; sodium amide Behandeln des Reaktionsgemisches mit Butylbromid, zuletzt bei Siedetemperatur;
参考文献
Baldinger; Nieuwland
Journal of the American Chemical Society, 1933 , vol. 55, p. 2851
反应条件
sodium hydroxide; polystyrene-bound benzyltrimethylammonium chloride T=80°C; 1.33333 h;
参考文献
Alvarez-Builla; Vaquero; Garcia Navio; Cabello; Sunkel; Fau De Casa-Juana; Dorrego; Santos
Tetrahedron, 1990 , vol. 46, # 3 p. 967 - 978
反应条件
sodium hydroxide; Silica D22; anhydrous tetramethylammonium chloride 18 h; Ambient temperature;
参考文献
Arrad, Onn; Sasson, Yoel
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2952 - 2954
反应条件
sodium hydroxide in dichloromethane T=20°C; 20 h;
参考文献
Badet, Bernard; Julia, Marc; Lefebvre, Christian
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 11-12 p. 431 - 434
