1-(4-吗啉基)-2-(4-吡啶基)乙硫酮合成路线 （共 8 条）
反应条件
sulfur Willgerodt-Kindler reaction; 0.0666667 h; microwave irradiation;
参考文献
Matloubi Moghaddam; Ghaffarzadeh
Synthetic Communications, 2001 , vol. 31, # 2 p. 317 - 321
反应条件
sulfur Willgerodt-Kindler reaction; 0.116667 h; microwave irradiation;
参考文献
Moghaddam, Firouz Matloubi; Ghaffarzadeh, Mohammad; Dakamin, Mohammad G.
Journal of Chemical Research - Part S, 2000 , # 5 p. 228 - 229
参考文献
Porter
Journal of the American Chemical Society, 1954 , vol. 76, p. 127
反应条件
1: ethanolic KOH 2: HCl View Scheme
参考文献
Malan; Dean
Journal of the American Chemical Society, 1947 , vol. 69, p. 1797
参考文献
Burger et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 3175
反应条件
sodium hydroxide 0.0166667 h; microwave irradiation;
参考文献
Matloubi Moghaddam; Ghaffarzadeh
Synthetic Communications, 2001 , vol. 31, # 2 p. 317 - 321
反应条件
1: 63.7 percent / potassium hydroxide / ethanol / 72 h / Heating 2: 1) potassium hydroxide; 2) conc hydrochloride acid / 1) aqueous EtOH, reflux, 72 h 2) reflux, 3 h View Scheme
参考文献
Labouta; Falch; Hjeds; Krogsgaard Larsen
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 6 p. 531 - 535
反应条件
1: 63.7 percent / potassium hydroxide / ethanol / 72 h / Heating 2: 1) potassium hydroxide; 2) conc hydrochloride acid / 1) aqueous EtOH, reflux, 72 h 2) reflux, 3 h 3: 58 percent / hydrogen / 5 percent Rh-Al2O3 / H2O / 20 h / 2250.2 Torr View Scheme
参考文献
Labouta; Falch; Hjeds; Krogsgaard Larsen
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 6 p. 531 - 535
