2-甲基-3-苯基-2-丙烯酰氯合成路线 （共 6 条）
反应条件
phosphorus trichoride; benzene
参考文献
Watanabe; Hayashi; Yoshimatsu; Sakai; Takeyama; Takashima
Journal of Medicinal Chemistry, 1980 , vol. 23, # 1 p. 50 - 59
反应条件
1: sodium, 2: thionyl chloride View Scheme
参考文献
Novrocik, Jan; Novrocikova, Marta
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 1 p. 60 - 70
反应条件
1: sodium acetate / 130 - 135 °C 2: benzene; PCl3 View Scheme
参考文献
Rupe; Busolt
Justus Liebigs Annalen der Chemie, 1909 , vol. 369, p. 320
反应条件
pyridine in benzene 12 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 4 p. 328 - 330
反应条件
1: ethyl acetate With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: (E)-2-Methyl-3-phenylpropenoyl chloride in tetrahydrofuran; hexane
T=-78°C;
参考文献
Aggarwal, Varinder K.; Belfield, Andrew J.
Organic Letters, 2003 , vol. 5, # 26 p. 5075 - 5078
反应条件
1: potassium carbonate / acetone
2: 92 percent / magnesium, methanol / Ambient temperature
View Scheme
参考文献
Brettle, Roger; Shibib, Sa'ad M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2912 - 2919
