3,5-二氯-N,N-二甲基苯胺合成路线 （共 11 条）
反应条件
methanol T=165 - 170°C;
参考文献
Astra Lakemedel Aktiebolag
Patent: US3996381 A1, 1976 ;
反应条件
hydrogenchloride; formaldehyd; sodium cyanoborohydride in water; acetic acid; acetone; acetonitrile
参考文献
Beecham Group P.L.C.
Patent: US4602041 A1, 1986 ;
反应条件
1: With N,N-dimethylthiocarbamoyl chloride in dichloromethane T=20°C; 2 h; 2: in acetonitrile 3 h; Reflux;
参考文献
Caliskan, Hafize; Zaim, Oemer
Synthetic Communications, 2010 , vol. 40, # 20 p. 3078 - 3083
反应条件
sodium hydride in tetrahydrofuran T=0 - 20°C;
参考文献
Li, Nan; Lim, Reyna K. V.; Edwardraja, Selvakumar; Lin, Qing
Journal of the American Chemical Society, 2011 , vol. 133, # 39 p. 15316 - 15319
反应条件
sodium tetrahydroborate; bis(cyclopentadienyl)titanium dichloride
参考文献
Liu, Yumin; Schwartz, Jeffrey
Tetrahedron, 1995 , vol. 51, # 15 p. 4471 - 4482
参考文献
Geigy and Co.
Patent: DE105103 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 5, p. 106
反应条件
nitric acid in acetic acid 0.0833333 h;
参考文献
Kriwanek, J.; Zemke, F.; Fanghaenel, E.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 2 p. 377 - 384
参考文献
Hodgson; Wignall
Journal of the Chemical Society, 1927 , p. 2218
Journal of the Chemical Society, 1928 , p. 331
参考文献
Hodgson; Wignall
Journal of the Chemical Society, 1927 , p. 2218
Journal of the Chemical Society, 1928 , p. 331
反应条件
trichlorophosphate in N-methyl-acetamide
参考文献
Astra Lakemedel Aktiebolag
Patent: US3996381 A1, 1976 ;
