2-丙-2-基氧羰基苯甲酸合成路线 （共 8 条）
参考文献
SALTIGO GMBH
Patent: US2012/16152 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
hydrogen fluoride; boron trifluoride
参考文献
Morin; Bearse
Industrial and Engineering Chemistry, 1951 , vol. 43, p. 1596,1598
参考文献
Suvorov,A.L.; Spasskii,S.S.
Doklady Chemistry, 1964 , vol. 157, p. 741 - 743
Doklady Akademii Nauk SSSR, 1964 , vol. 157, # 3 p. 639 - 642
反应条件
water var. ratio of solvents; Rate constant;
参考文献
Mollin, Jiri; Pavelek, Zdenek; Kasparek, Frantisek
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 5 p. 1115 - 1130
反应条件
copper(I) oxide; 1,10-phenanthroline in 1-methyl-pyrrolidin-2-one; quinoline T=190°C; 0.0833333 h; Microwave irradiation;
参考文献
Goossen, Lukas J.; Manjolinho, Filipe; Khan, Bilal A.; Rodriguez, Nuria
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2620 - 2623
反应条件
copper(I) oxide; 1,10-phenanthroline in 1-methyl-pyrrolidin-2-one; quinoline T=170°C; 12 h; Product distribution;
参考文献
Goossen, Lukas J.; Thiel, Werner R.; Rodriguez, Nuria; Linder, Christophe; Melzer, Bettina
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 14-15 p. 2241 - 2246
反应条件
1.1: potassium hydroxide / isopropyl alcohol / 1 h / 20 °C 2.1: 1,10-phenanthroline; copper(II) oxide / 2-dicyclohexylphosphino-1,1'-biphenyl; palladium (II) 2,4-pentanedionate / 1 h / Reflux 2.2: 16 h / 180 °C / Inert atmosphere 3.1: potassium hydroxide / 1-methyl-pyrrolidin-2-one / 20 - 95 °C / Reflux 3.2: 3 h / 10 - 20 °C / pH 1 - 2 View Scheme
参考文献
SALTIGO GMBH
Patent: US2012/16152 A1, 2012 ;
反应条件
hydrogen fluoride; boron trifluoride
参考文献
Morin; Bearse
Industrial and Engineering Chemistry, 1951 , vol. 43, p. 1596,1598
