N-吗啉-4-甲基苯磺酰胺合成路线 （共 15 条）
反应条件
tetrafluoroboric acid; K2S2O5; tetrabutylammomium bromide; palladium diacetate; [(t-Bu)3PH]BF4 in 1,4-dioxane T=80°C; 12 h; Reagent/catalystSolventTemperature;
参考文献
Ye, Shengqing; Wu, Jie
Chemical Communications, 2012 , vol. 48, # 80 p. 10037 - 10039
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate; [(t-Bu)3PH]BF4 in 1,4-dioxane T=70°C; 16 h; Inert atmosphere;
参考文献
Emmett, Edward J.; Richards-Taylor, Charlotte S.; Nguyen, Bao; Garcia-Rubia, Alfonso; Hayter, Barry R.; Willis, Michael C.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 20 p. 4007 - 4014
反应条件
(DABCO)*(SO2)2; palladium diacetate; [(t-Bu)3PH]BF4 in 1,4-dioxane T=90°C; 16 h; Inert atmosphere;
参考文献
Emmett, Edward J.; Richards-Taylor, Charlotte S.; Nguyen, Bao; Garcia-Rubia, Alfonso; Hayter, Barry R.; Willis, Michael C.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 20 p. 4007 - 4014
反应条件
DABCO-bis(sulfur dioxide); tetrabutylammomium bromide; oxygen; palladium diacetate in 1,4-dioxane T=80°C; 12 h;
参考文献
Ye, Shengqing; Wu, Jie
Chemical Communications, 2012 , vol. 48, # 62 p. 7753 - 7755
反应条件
DABCO-bis(sulfur dioxide) in acetonitrile T=25°C; 0.333333 h; Inert atmosphere;
参考文献
Zheng, Danqing; An, Yuanyuan; Li, Zhenhua; Wu, Jie
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2451 - 2454
Angew. Chem., 2014 , vol. 126, # 9 p. 2483 - 2486,4
反应条件
1.1: DABCO-bis(sulfur dioxide) / tetrahydrofuran / 1 h / -40 °C / Inert atmosphere 1.2: -40 - 20 °C / Inert atmosphere 2.1: tetrahydrofuran / 3 h / 20 °C / Inert atmosphere View Scheme
参考文献
Woolven, Holly; Gonzalez-Rodriguez, Carlos; Marco, Isabel; Thompson, Amber L.; Willis, Michael C.
Organic Letters, 2011 , vol. 13, # 18 p. 4876 - 4878
反应条件
in tetrahydrofuran T=20°C; 3 h; Inert atmosphere;
参考文献
Woolven, Holly; Gonzalez-Rodriguez, Carlos; Marco, Isabel; Thompson, Amber L.; Willis, Michael C.
Organic Letters, 2011 , vol. 13, # 18 p. 4876 - 4878
反应条件
1: 4-methyl-N-morpholin-4-ylbenzenesulfonamide With benzyl bromide; potassium carbonate in 1,4-dioxane T=50°C; 1 h; 2: Diphenyliodonium triflate T=100°C; 15 h;
参考文献
Richards-Taylor, Charlotte S.; Blakemore, David C.; Willis, Michael C.
Chemical Science, 2013 , vol. 5, # 1 p. 222 - 228
反应条件
potassium carbonate in 1,4-dioxane T=100°C;
参考文献
Richards-Taylor, Charlotte S.; Blakemore, David C.; Willis, Michael C.
Chemical Science, 2013 , vol. 5, # 1 p. 222 - 228
反应条件
potassium carbonate in 1,4-dioxane
T=100°C;
参考文献
Richards-Taylor, Charlotte S.; Blakemore, David C.; Willis, Michael C.
Chemical Science, 2013 , vol. 5, # 1 p. 222 - 228
