2-戊基-1,3-二氧戊环合成路线 （共 13 条）
反应条件
naphthalene; lithium in tetrahydrofuran T=-78°C; 2.5 h;
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Anales de Quimica, 1998 , vol. 94, # 1 p. 56 - 61
反应条件
di-tert-butyl peroxide T=175°C; P=147102 Torr;
参考文献
Foster et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 5606,5608
反应条件
sodium hydrogencarbonate; toluene-4-sulfonic acid in ethylene glycol; benzene
参考文献
Macro Chem. Corp.
Patent: US4861764 A1, 1989 ;
反应条件
distannoxane 1a in benzene 0.5 h; Heating;
参考文献
Otera, Junzo; Dan-oh, Nobuhisa; Nozaki, Hitosi
Tetrahedron, 1992 , vol. 48, # 8 p. 1449 - 1456
反应条件
distannoxane 1a in benzene 0.5 h; Heatingother distannoxane catalysts, other aldehydes, other alcohol, other solvents, other reaction times; MechanismProduct distribution;
参考文献
Otera, Junzo; Dan-oh, Nobuhisa; Nozaki, Hitosi
Tetrahedron, 1992 , vol. 48, # 8 p. 1449 - 1456
反应条件
1: 65 percent / sodium acetate, pyridinium chlorochromate / CH2Cl2 / 1.5 h / Ambient temperature 2: 93 percent / p-toluenesulfonic acid / toluene / 2 h / Heating 3: 92 percent / Li, naphthalene / tetrahydrofuran / 2.5 h / -78 °C View Scheme
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Anales de Quimica, 1998 , vol. 94, # 1 p. 56 - 61
反应条件
1: 93 percent / p-toluenesulfonic acid / toluene / 2 h / Heating 2: 92 percent / Li, naphthalene / tetrahydrofuran / 2.5 h / -78 °C View Scheme
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Anales de Quimica, 1998 , vol. 94, # 1 p. 56 - 61
反应条件
T=175°C; P=147102 Torr;
参考文献
Foster et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 5606,5608
反应条件
CoCl2.6H2O; zinc in tetrahydrofuran T=20°C; 5 h;
参考文献
Sarma, Kuladip; Goswami, Amrit
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 568 - 572
反应条件
methanol; manganese(IV) oxide; chloro-trimethyl-silane; manganese (II) chloride in acetonitrile T=40°C; 6 h;
参考文献
Tetrahedron, , vol. 48, # 22 p. 4579 - 4586
