(Z)-5-十四碳烯-1-醇乙酸酯合成路线 （共 19 条）
反应条件
2: 90 percent / lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature 3: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
反应条件
1: 86 percent / dimethylsulfoxide / Ambient temperature 2: KOH / ethane-1,2-diol / 6 h / Heating 4: 90 percent / lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature 5: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
反应条件
1: KOH / ethane-1,2-diol / 6 h / Heating 3: 90 percent / lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature 4: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
反应条件
1: triethylamine / CH2Cl2 / 1) 0 deg C, 0.5 h, 2) RT, 6 h 2: LiBr / acetone / 5 h / Ambient temperature 3: 86 percent / dimethylsulfoxide / Ambient temperature 4: KOH / ethane-1,2-diol / 6 h / Heating 6: 90 percent / lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature 7: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
反应条件
1: LiBr / acetone / 5 h / Ambient temperature 2: 86 percent / dimethylsulfoxide / Ambient temperature 3: KOH / ethane-1,2-diol / 6 h / Heating 5: 90 percent / lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature 6: 74 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
反应条件
1: -78 °C 2: 1.)9-Borabicyclononan, 2.)H2O2/OH(-) 3: 76 percent / pyridin View Scheme
参考文献
Bestmann, H. J.; Brosche, T.; Koschatzky, K. H.; Michaelis, K.; Platz, H.; et. al.
Tetrahedron Letters, 1980 , vol. 21, p. 747 - 750
反应条件
1: 1.)9-Borabicyclononan, 2.)H2O2/OH(-) 2: 76 percent / pyridin View Scheme
参考文献
Bestmann, H. J.; Brosche, T.; Koschatzky, K. H.; Michaelis, K.; Platz, H.; et. al.
Tetrahedron Letters, 1980 , vol. 21, p. 747 - 750
反应条件
1: -78 °C 2: 1.)9-Borabicyclononan, 2.)H2O2/OH(-) 3: 76 percent / pyridin View Scheme
参考文献
Bestmann, H. J.; Brosche, T.; Koschatzky, K. H.; Michaelis, K.; Platz, H.; et. al.
Tetrahedron Letters, 1980 , vol. 21, p. 747 - 750
反应条件
1: NaN<Si(CH3)3>2 2: -78 °C 3: 1.)9-Borabicyclononan, 2.)H2O2/OH(-) 4: 76 percent / pyridin View Scheme
参考文献
Bestmann, H. J.; Brosche, T.; Koschatzky, K. H.; Michaelis, K.; Platz, H.; et. al.
Tetrahedron Letters, 1980 , vol. 21, p. 747 - 750
