3,4-二甲氧基苯乙基异氰酸酯合成路线 （共 18 条）
参考文献
Lebedev; Lebedeva; Sheludyakov; Ovcharuk; Kovaleva; Ustinova
Russian Journal of General Chemistry, 2006 , vol. 76, # 3 p. 469 - 477
反应条件
alpha-chloropyridine; trifluoromethylsulfonic anhydride in dichloromethane T=-78°C; 0.5 h; Inert atmosphere; regioselective reaction;
参考文献
In, Jinkyung; Hwang, Soonho; Kim, Changhun; Seo, Jae Hong; Kim, Sanghee
European Journal of Organic Chemistry, 2013 , # 5 p. 965 - 971
参考文献
Judd, Katie E.; Mahon, Mary F.; Caggiano, Lorenzo
Synthesis, 2009 , # 16 p. 2809 - 2817
反应条件
1: NaN3 / acetone; H2O 2: benzene / Heating View Scheme
参考文献
Fries; Bestian
Justus Liebigs Annalen der Chemie, 1938 , vol. 533, p. 72,83
反应条件
1: SOCl2 2: NaN3 / acetone; H2O 3: benzene / Heating View Scheme
参考文献
Fries; Bestian
Justus Liebigs Annalen der Chemie, 1938 , vol. 533, p. 72,83
反应条件
1: 93.6 percent / H2SO4 / 2 h / Heating 2: 77.3 percent / toluene / 0 °C View Scheme
参考文献
Lebedev; Lebedeva; Sheludyakov; Ovcharuk; Kovaleva; Ustinova
Russian Journal of General Chemistry, 2006 , vol. 76, # 3 p. 469 - 477
反应条件
in toluene T=100°C; Cooling with ice;
参考文献
Wang, Liutang; Zhang, Bin; Ji, Jianxin; Li, Bogang; Yan, Jufang; Zhang, Weiyu; Wu, Yong; Wang, Xuechao; Hou, Hui
Synthetic Communications, 2010 , vol. 40, # 1 p. 52 - 57
反应条件
1: benzene; hydrazine hydrate 2: aqueous hydrochloric acid; aqueous sodium nitrite solution 3: benzene View Scheme
参考文献
Mohunta; Ray
Journal of the Chemical Society, 1934 , p. 1263
反应条件
1: aqueous hydrochloric acid; aqueous sodium nitrite solution 2: benzene View Scheme
参考文献
Mohunta; Ray
Journal of the Chemical Society, 1934 , p. 1263
参考文献
Fries; Bestian
Justus Liebigs Annalen der Chemie, 1938 , vol. 533, p. 72,83
