1,4-双(溴甲基)-2,5-二甲苯合成路线 （共 10 条）
反应条件
hydrogen bromide; tetradecyltrimethylammonium bromide; acetic acid 24 h; Heating;
参考文献
Pischel, Ivo; Nieger, Martin; Archut, Andreas; Voegtle, Fritz
Tetrahedron, 1996 , vol. 52, # 30 p. 10043 - 10052
反应条件
hydrogen bromide T=100°C;
参考文献
Chemische Berichte, , vol. 67, p. 1094,1096
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane Bromination;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 8, # 5 p. 1041 - 1058
反应条件
hydrogen bromide; acetic acid T=60°C; 24 h;
参考文献
Kawashima, Hirotsugu; Kawabata, Kohsuke; Goto, Hiromasa
Journal of Polymer Science, Part A: Polymer Chemistry, 2012 , vol. 50, # 8 p. 1530 - 1538
反应条件
1: BH3*THF 2: 48percent aq. HBr, Ac2O View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 2 p. 366 - 378
反应条件
2: glacial acetic acid 3: alkaline solution 4: concentrated aqueous HBr / 100 °C View Scheme
参考文献
Chemische Berichte, , vol. 67, p. 1094,1096
反应条件
1: alkaline solution 2: concentrated aqueous HBr / 100 °C View Scheme
参考文献
Chemische Berichte, , vol. 67, p. 1094,1096
反应条件
1: glacial acetic acid 2: alkaline solution 3: concentrated aqueous HBr / 100 °C View Scheme
参考文献
Chemische Berichte, , vol. 67, p. 1094,1096
反应条件
N-bromosuccinmide; chloroform; dibenzoyl peroxide Irradiation.Gluehlampenlicht;
参考文献
Searle and Co.
Patent: US2865964 , 1955 ;
反应条件
sodium hydroxide; thiourea
1.) 95percent ethanol, reflux, 5 h, 2.) ethanol, reflux, 5 h; Yield given. Multistep reaction;
参考文献
Pischel, Ivo; Nieger, Martin; Archut, Andreas; Voegtle, Fritz
Tetrahedron, 1996 , vol. 52, # 30 p. 10043 - 10052
