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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯甲砜
合成路线
（共 34 条）
1879-16-9
4-甲氧基茴香硫醚
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Yang, Chuanbo; Jin, Qingping; Zhang, Hua; Liao, Jian; Zhu, Jin; Yu, Bin; Deng, Jingen
Green Chemistry, 2009 , vol. 11, # 9 p. 1401 - 1405
1879-16-9
4-甲氧基茴香硫醚
→
反应条件
3517-90-6
4-甲氧基苯甲砜
+
3517-99-5
反应条件
phosphate buffer; dihydrogen peroxide; chiral Al(salalen) in methanol T=20°C; 24 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 25 p. 4729 - 4731
5720-07-0
4-甲氧基苯硼酸
+
20277-69-4
甲烷亚磺酸钠
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
copper(I) oxide; ammonium hydroxide; oxygen in water T=25°C; 48 h;
参考文献
Yang, Haijun; Li, Yong; Jiang, Min; Wang, Junmei; Fu, Hua
Chemistry - A European Journal, 2011 , vol. 17, # 20 p. 5652 - 5660
1879-16-9
4-甲氧基茴香硫醚
→
反应条件
反应条件
dihydrogen peroxide; (Ra,S,S,Ra)-Al(salalen) in phosphate buffer; toluene T=0°C; pH=7.4; 25 h;
参考文献
Matsumoto, Kazuhiro; Yamaguchi, Tetsufumi; Katsuki, Tsutomu
Chemical Communications, 2008 , # 14 p. 1704 - 1706
696-62-8
4-碘苯甲醚
+
20277-69-4
甲烷亚磺酸钠
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
copper(l) iodide in dimethyl sulfoxide 24 h; Heating;
参考文献
Shen, Chao; Xu, Jun; Yu, Wenbo; Zhang, Pengfei
Green Chemistry, 2014 , vol. 16, # 6 p. 3007 - 3012
1879-16-9
4-甲氧基茴香硫醚
→
反应条件
3517-90-6
4-甲氧基苯甲砜
+
3517-99-5
反应条件
titanium(IV) isopropylate; 4 A molecular sieve; chiral 2-hydroperoxy-2-(2'-furil)bicyclo-[2.2.1]heptane in toluene T=-20°C; 4 h;
参考文献
Lattanzi, Alessandra; Iannece, Patrizia; Scettri, Arrigo
Tetrahedron Asymmetry, 2004 , vol. 15, # 11 p. 1779 - 1785
104-92-7
4-溴苯甲醚
+
20277-69-4
甲烷亚磺酸钠
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
copper(l) iodide; sodium (SC)-prolinate in dimethyl sulfoxide T=95°C; 36 h;
参考文献
Zhu, Wei; Ma, Dawei
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2696 - 2700
696-62-8
4-碘苯甲醚
+
74-88-4
甲基碘
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
1: para-iodoanisole With 1,10-phenanthroline; K2S2O5; tetrabutylammomium bromide; sodium formate; palladium diacetate; triphenylphosphine in dimethyl sulfoxide T=70°C; 2 h; Inert atmosphereMicrowave irradiation; 2: methyl iodide in dimethyl sulfoxide T=23°C; 20 h; Inert atmosphere; Reagent/catalystSolvent; chemoselective reaction;
参考文献
Shavnya, Andrei; Coffey, Steven B.; Smith, Aaron C.; Mascitti, Vincent
Organic Letters, 2013 , vol. 15, # 24 p. 6226 - 6229
104-92-7
4-溴苯甲醚
+
74-88-4
甲基碘
→
反应条件
3517-90-6
4-甲氧基苯甲砜
反应条件
1: 1-bromo-4-methoxy-benzene With 1,10-phenanthroline; K2S2O5; tetrabutylammomium bromide; sodium formate; palladium diacetate; triphenylphosphine in dimethyl sulfoxide T=70°C; 20 h; Inert atmosphereMicrowave irradiation; 2: methyl iodide in dimethyl sulfoxide T=23°C; 20 h; Inert atmosphere; Solvent; chemoselective reaction;
参考文献
Shavnya, Andrei; Coffey, Steven B.; Smith, Aaron C.; Mascitti, Vincent
Organic Letters, 2013 , vol. 15, # 24 p. 6226 - 6229
1879-16-9
4-甲氧基茴香硫醚
→
反应条件
3517-90-6
4-甲氧基苯甲砜
+
93381-75-0
+
93381-76-1
反应条件
titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate in dichloromethane T=-17°C; 6.5 h; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 106, # 26 p. 8188 - 8193
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