反应条件
in hexane
under Ar, soln. of N,N-diethylcrotonamide in hexane cooled to -60°C, soln. of Et3GeLi in hexane added dropwise, stirred for 3 h at -60°C, quenched with methanol; washed with satd. soln. of NH4Cl, dried (MgSO4), evapd., distd.; elem. anal.;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 51 - 60
