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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
35190-16-0
合成路线
（共 10 条）
89-98-5
2-氯苯甲醛
→
反应条件
35190-16-0
反应条件
thiamine chloride hydrochloride; triethylamine in water pH=8.5; 0.00555556 h; microwave irradiation;
参考文献
Bag, Seema; Vaze, Vidula V.; Degani, Mariam S.
Journal of Chemical Research, 2006 , # 4 p. 267 - 269
89-98-5
2-氯苯甲醛
+
292638-85-8
丙烯酸甲酯
→
反应条件
反应条件
1: 2-chloro-benzaldehyde With potassium tert-butylate; [mmim][I] in tetrahydrofuran T=20°C; 3 h; 2: acrylic acid methyl ester in tetrahydrofuran T=20°C; 8 h;
参考文献
Ye, Wei; Cai, Guanliang; Zhuang, Zeyang; Jia, Xueshun; Zhai, Hongbin
Organic Letters, 2005 , vol. 7, # 17 p. 3769 - 3771
21854-95-5
2,2'-二氯联苯甲酰
→
反应条件
35190-16-0
反应条件
hydroxymethanesulfinic acid sodium salt in water; N,N-dimethyl-formamide T=100°C; 1 h;
参考文献
Harris, Alan R.; Mason, Timothy J.
Synthetic Communications, 1989 , vol. 19, # 3and4 p. 529 - 536
89-98-5
2-氯苯甲醛
+
101-39-3
α-甲基肉桂醛
→
反应条件
反应条件
benzaldehyde lyase from Pseudomonas fluorescens; thiamine diphosphate; magnesium chloride in dimethyl sulfoxide T=20°C; pH=7.0; 168 h; aq. phosphate bufferInert atmosphereEnzymatic reaction; optical yield given as percent ee;
参考文献
Cosp, Anabel; Dresen, Carola; Pohl, Martina; Walter, Lydia; Roehr, Caroline; Mueller, Michael
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 5 p. 759 - 771
89-98-5
2-氯苯甲醛
+
104-55-2
肉桂醛
→
反应条件
反应条件
benzaldehyde lyase from Pseudomonas fluorescens; thiamine diphosphate; magnesium chloride in dimethyl sulfoxide T=20°C; pH=7.0; 48 h; aq. phosphate bufferInert atmosphereEnzymatic reaction;
参考文献
Cosp, Anabel; Dresen, Carola; Pohl, Martina; Walter, Lydia; Roehr, Caroline; Mueller, Michael
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 5 p. 759 - 771
104-53-0
苯丙醛
+
89-98-5
2-氯苯甲醛
→
反应条件
1256164-91-6
+
1256164-60-9
+
35190-16-0
反应条件
Rb2CO3; 2-pentafluorophenyl-6,17dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate in tetrahydrofuran T=20°C; acyloin condensation; 40 h; Inert atmosphere; chemoselective reaction;
参考文献
O'Toole, Sarah E.; Rose, Christopher A.; Gundala, Sivaji; Zeitler, Kirsten; Connon, Stephen J.
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 347 - 357
21854-95-5
2,2'-二氯联苯甲酰
→
反应条件
35190-16-0
反应条件
hydrogen iodide; acetic acid
参考文献
Huang; Lee
Journal of the Chemical Society, 1959 , p. 923,927
35190-16-0
→
反应条件
21854-95-5
2,2'-二氯联苯甲酰
反应条件
urea hydrogen peroxide addition compound; lanthanum trifluoromethanesulphonate T=70°C; 0.833333 h; Ionic liquidGreen chemistry;
参考文献
Saluja, Pooja; Magoo, Devanshi; Khurana, Jitender M.
Synthetic Communications, 2014 , vol. 44, # 6 p. 800 - 806
35190-16-0
→
反应条件
89405-42-5
反应条件
1: SOCl2 2: ethanol / 6 h / Heating 3: 70 percent / piperidine / ethanol / 1 h / Heating View Scheme
参考文献
Dash; Patra; Mahapatra
Journal of the Indian Chemical Society, 1983 , vol. 60, # 8 p. 772 - 774
35190-16-0
→
反应条件
89405-44-7
反应条件
1: SOCl2 2: ethanol / 6 h / Heating View Scheme
参考文献
Dash; Patra; Mahapatra
Journal of the Indian Chemical Society, 1983 , vol. 60, # 8 p. 772 - 774
