4,4'-二硫代二苯甲酸二甲酯合成路线 （共 15 条）
参考文献
Miles Inc.
Patent: US5266713 A1, 1993 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether 1 h; Ambient temperature;
参考文献
Itoh, Takahito; Gotoh, Kenji; Ishikawa, Noriyuki; Hamaguchi, Tosisige; Kubo, Masataka
Journal of Organic Chemistry, 1996 , vol. 61, # 5 p. 1867 - 1869
反应条件
acetic acid; zinc 4 h; Heating;
参考文献
Werbel; Newton; Elslager
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 3 p. 497 - 500
反应条件
ammonia; sodium
1.) -50 deg C to -30 deg C, 2.) DMF, 22 deg C - 30 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Boiko, V. N.; Shchupak, G. M.
Journal of Fluorine Chemistry, 1994 , vol. 69, # 3 p. 207 - 212
反应条件
pyridine; sulfuryl dichloride in dichloromethane
0.166667 h;
参考文献
BETA PHARMA CANADA INC.; WANG, Zhaoyin; LI, Lianhai
Patent: WO2013/78544 A1, 2013 ;
Location in patent: Paragraph 00113-00114 ;
