反应条件
1.1: magnesium / tetrahydrofuran / |Reflux
1.2: 24 h / |Reflux
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate / pyridine / 2.5 h / 0 - 80 °C
3.1: palladium 10 on activated carbon; hydrogen / ethyl acetate; methanol / 5 h / 30003 Torr
4.1: tetrahydrofuran; water; sulfuric acid / 1.5 h
View Scheme
参考文献
Zhou, Lin; Liu, Xiaohua; Ji, Jie; Zhang, Yuheng; Hu, Xiaolei; Lin, Lili; Feng, Xiaoming
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 20208 - 20208
