4-(三氟甲基硫代)甲苯合成路线 （共 35 条）
反应条件
[Ni0(1,5-cyclooctadiene)2]; 4,4'-dimethoxy-2,2'-bipyridine in tetrahydrofuran T=20°C; 22 h; Inert atmosphere;
参考文献
Zhang, Cheng-Pan; Vicic, David A.
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 183 - 185
反应条件
1: 4-toluenediazonium tetrafluoroborate With copper(I) isothiocyanate; sodium isothiocyanate; caesium carbonate in acetonitrile T=20°C; 0.166667 h; Inert atmosphere; 2: (trifluoromethyl)-trimethylsilane in acetonitrile T=20°C; 16 h;
参考文献
Chemical Science, , vol. 5, # 4 p. 1312 - 1316
反应条件
hydrogen fluoride T=100 - 160°C;
参考文献
US2108606 , ;
DE682971 , ;
DRP/DRBP Org.Chem.
反应条件
sulfur; N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(l) iodide T=100°C; 7 h;
参考文献
Chen, Qing-Yun; Duan, Jian-Xing
Journal of the Chemical Society, Chemical Communications, 1993 , # 11 p. 918 - 919
反应条件
in N,N-dimethyl-formamide 240 h; Irradiation;
参考文献
Naumann, D.; Pazenok, S. V.; Turra, V.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.2 p. 128 - 130
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 152 - 155
反应条件
in trifluoroacetic acid T=50 - 60°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 29, p. 297
反应条件
boron trifluoride 100°C; 4 h; in autoclave;
参考文献
Journal of Organic Chemistry, , vol. 29, p. 898 - 900
参考文献
Journal of Organic Chemistry, , vol. 29, p. 895 - 898
反应条件
in water; acetone byproducts: N2;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.10, page 251 - 267
反应条件
in ammonia Irradiationvar.solv.: DMF; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 29, p. 210
