N-(2,6-二乙基苯基)甲亚胺合成路线 (共 12 条)
反应条件
trimethylamine; paraformaldehyde in n-heptane
参考文献
Velsicol Chemical Corporation
Patent: US3976471 A1, 1976 ;
反应条件
2 h; Ambient temperature;
参考文献
Pastushenko, E. V.; Safiulova, G. I.; Kruglov, D. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 11.2 p. 2143 - 2148
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 11 p. 2412 - 2418
反应条件
N-(chloromethyl)-2,6-diethylcarbaniloyl chloride in acetone 1.) reflux, 5 h; 2.) 25-30 deg C, 18 h; Yield given;
参考文献
D'Amico, John J.; Bollinger, Frederic G.; Tung, Ching C.; Dahl, William E.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 945 - 948
反应条件
N-(chloromethyl)-2,6-diethylcarbaniloyl chloride in acetone 1.) reflux, 5 h; 2.) 25-30 deg C, 18 h; Yield given;
参考文献
D'Amico, John J.; Bollinger, Frederic G.; Tung, Ching C.; Dahl, William E.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 945 - 948
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Giumanini, Angelo G.; Verardo, Giancarlo; Polana, Marco
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 2 p. 161 - 174
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Giumanini, Angelo G.; Verardo, Giancarlo; Polana, Marco
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 2 p. 161 - 174
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 330, # 2 p. 161 - 174
反应条件
in acetone Ambient temperature; Further byproducts given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 5.2 p. 807 - 809
Zhurnal Organicheskoi Khimii, , vol. 28, # 5 p. 1039 - 1041
反应条件
in acetone Ambient temperature; Further byproducts given;
参考文献
Terent'ev, A. B.; Yashkina, L. V.; Pastushenko, E. V.; Kruglov, D. E.; Safiulova, G. I.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 5.2 p. 807 - 809
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 5 p. 1039 - 1041
反应条件
in acetone Ambient temperature; Further byproducts given;
参考文献
Terent'ev, A. B.; Yashkina, L. V.; Pastushenko, E. V.; Kruglov, D. E.; Safiulova, G. I.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 5.2 p. 807 - 809
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 5 p. 1039 - 1041