六氢化-1,3,5-三(1-氧代-2-丙烯基)-1,3,5-三嗪合成路线 （共 16 条）
反应条件
tripotassium phosphate monohydrate; dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran; water T=60°C; 24 h;
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS; BURKE, Martin, D.; KNAPP, David, M.; GILLIS, Eric, P.
Patent: WO2010/36921 A2, 2010 ;
Location in patent: Page/Page column 65-66 ;
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; potassium carbonate; PdI2 in water; isopropyl alcohol T=80°C; Suzuki reaction; 5 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
反应条件
lithium chloride; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; N,N-dimethyl-formamide T=80°C; Stille coupling; 22 h;
参考文献
Hoshino, Masahide; Degenkolb, Peter; Curran, Dennis P.
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8341 - 8349
反应条件
potassium carbonate; N,N-diethylaminopropyl-Al2O3-Pd(OAc)2 in ethanol; water T=80°C; Suzuki-Miyaura reaction; 5 h; microwave irradiation;
参考文献
Hagiwara, Hisahiro; Keon, Hyeok Ko; Hoshi, Takashi; Suzuki, Toshio
Synlett, 2008 , # 4 p. 611 - 613
反应条件
bis[di(tert-butyl)chlorophosphine]palladium dichloride in acetonitrile T=82°C; Stille cross-coupling;
参考文献
Lerebours, Rachel; Camacho-Soto, Alexandra; Wolf, Christian
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8601 - 8604
反应条件
palladium diacetate; sodium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in ethanol T=85°C; Suzuki-Miyaura coupling; 16 h; Inert atmosphere;
参考文献
Molander, Gary A.; Canturk, Belgin; Kennedy, Lauren E.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 973 - 980
反应条件
1: 2-Furan-2-yl-4,5-dimethyl-[1,3,2]dioxaborolane With NiCl2((PPh3)P)2; methyllithium in tetrahydrofuran T=20°C; 0.25 h; 2: 4-methanesulfonyloxyacetophenone in tetrahydrofuran T=20°C; 12 h;
参考文献
Kobayashi, Yuichi; William, Anthony D.; Mizojiri, Ryo
Journal of Organometallic Chemistry, 2002 , vol. 653, # 1-2 p. 91 - 97
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; water T=20°C; 12 h;
参考文献
Pena-Lopez, Miguel; Sarandeses, Luis A.; Perez Sestelo, Jose
European Journal of Organic Chemistry, 2013 , # 13 p. 2545 - 2554
反应条件
palladium 10 on activated carbon; LiF in 1-methyl-pyrrolidin-2-one T=120°C; Stille coupling; 24 h;
参考文献
Yabe, Yuki; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2010 , vol. 66, # 45 p. 8654 - 8660
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in tetrahydrofuran; N,N-dimethyl-formamide T=80°C; 22 h;
参考文献
Curran, Dennis P.; Hoshino, Masahide
Journal of Organic Chemistry, 1996 , vol. 61, # 19 p. 6480 - 6481
