5-氯四唑并[1,5-a]吡啶合成路线 (共 3 条)
反应条件
1: alpha-chloropyridine With fluorine in chloroform T=-78 - -60°C; 2: p-(trifluoromethyl)phenyl isonitrile With trimethylsilylazide in chloroform T=-50 - 0°C;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 29 p. 4851 - 4854
反应条件
hydrogenchloride; sodium nitrite pH=1;
参考文献
Reisinger, Ales; Bernhardt, Paul V.; Wentrup, Curt
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 2 p. 246 - 256
反应条件
1: 78 percent / hydrazine hydrate / ethanol / 80 - 90 °C 2: 69.8 percent / aq. HCl; NaNO2 / pH 1 View Scheme
参考文献
Reisinger, Ales; Bernhardt, Paul V.; Wentrup, Curt
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 2 p. 246 - 256