1-Boc-5-氟吲哚-2-硼酸合成路线 （共 3 条）
反应条件
1: With tri-isopropoxy-borane; lithium diisopropyl amide in tetrahydrofuran T=0°C; 2 h; 2: With phosphate buffer in tetrahydrofuran pH=6.0; Further stages.;
参考文献
Mizuta, Masahiro; Seio, Kohji; Miyata, Kenichi; Sekine, Mitsuo
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5046 - 5055
反应条件
1.1: 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 1 h / 20 °C 2.1: triisopropyl borate; LDA / tetrahydrofuran / 2 h / 0 °C 2.2: 98 percent / aq. phosphate buffer / tetrahydrofuran / pH 6.0 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 14 p. 5046 - 5055
反应条件
1.1: 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 1 h / 20 °C 2.1: triisopropyl borate; LDA / tetrahydrofuran / 2 h / 0 °C 2.2: 98 percent / aq. phosphate buffer / tetrahydrofuran / pH 6.0 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 14 p. 5046 - 5055
