9-甲氧基-alpha-拉帕醌合成路线 （共 5 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol 1 h; Ambient temperature;
参考文献
Tapia, Ricardo; Valderrama, Jaime A.; Quintanar, Carmina
Heterocycles, 1994 , vol. 38, # 8 p. 1797 - 1804
反应条件
1: 83 percent / methanol / 1 h / Ambient temperature 2: 1.) NaH, 2.) Ag2O, MgSO4 / 1.) THF, 0 deg C, 30 min, 2.) THF, 1.5 h 3: 83 percent / p-toluenesulfonic acid / xylene / 1.25 h / Heating 4: 99 percent / H2 / 10percent Pd/C / ethanol / 1 h / Ambient temperature View Scheme
参考文献
Tapia, Ricardo; Valderrama, Jaime A.; Quintanar, Carmina
Heterocycles, 1994 , vol. 38, # 8 p. 1797 - 1804
反应条件
1: 83 percent / methanol / 1 h / Ambient temperature 2: 1.) NaH, 2.) Ag2O, MgSO4 / 1.) THF, 0 deg C, 30 min, 2.) THF, 1.5 h 3: 83 percent / p-toluenesulfonic acid / xylene / 1.25 h / Heating 4: 99 percent / H2 / 10percent Pd/C / ethanol / 1 h / Ambient temperature View Scheme
参考文献
Tapia, Ricardo; Valderrama, Jaime A.; Quintanar, Carmina
Heterocycles, 1994 , vol. 38, # 8 p. 1797 - 1804
反应条件
1: 1.) NaH, 2.) Ag2O, MgSO4 / 1.) THF, 0 deg C, 30 min, 2.) THF, 1.5 h 2: 83 percent / p-toluenesulfonic acid / xylene / 1.25 h / Heating 3: 99 percent / H2 / 10percent Pd/C / ethanol / 1 h / Ambient temperature View Scheme
参考文献
Tapia, Ricardo; Valderrama, Jaime A.; Quintanar, Carmina
Heterocycles, 1994 , vol. 38, # 8 p. 1797 - 1804
反应条件
potassium carbonate in acetone
参考文献
Kapoor, N. K.; Gupta, R. B.; Khanna, R. N.
Tetrahedron Letters, 1980 , vol. 21, p. 5083 - 5084
