2-(丁烷-2-基氨基)乙醇合成路线 (共 5 条)
反应条件
in methanol T=20°C; 4 h;
参考文献
Bayer Corporation
Patent: US6353006 B1, 2002 ;
Location in patent: Page column 37 ;
US 6353006 B1
反应条件
ethanol; platinum T=150°C; P=140 - 51485.6 Torr; Hydrogenation;
参考文献
Cope; Hancock
Journal of the American Chemical Society, 1942 , vol. 64, p. 1503,1504
反应条件
1: With titanium(IV) isopropylate in tetrahydrofuran T=20°C; 8 h; 2: With sodium tetrahydroborate in tetrahydrofuran; ethanol T=20°C; 8 h;
参考文献
Kumpaty, Hephzibah J.; Bhattacharyya, Sukanta; Rehr, Erik W.; Gonzalez, Amelia M.
Synthesis, 2003 , # 14 p. 2206 - 2210
反应条件
sodium tetrahydroborate in ethanol T=0°C; 0.0833333 h; Yield given;
参考文献
Saavedra, Joseph E.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2271 - 2273
反应条件
potassium hydroxide HeatingCH3ONa as reagent;
参考文献
Kukharev, B.F.; Stankevich, V.K.; Kukhareva, V.A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 437 - 439
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 533 - 535