(4-硝基苯基)-丙酸乙酯合成路线 （共 18 条）
反应条件
potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran 16 h; Heating / reflux;
参考文献
AstraZeneca AB
Patent: US7081461 B1, 2006 ;
Location in patent: Page/Page column 38 ;
US 7081461 B1
反应条件
tetraethylammonium chloride; bis-triphenylphosphine-palladium(II) chloride in benzene T=50°C; 1 h;
参考文献
Sakamoto; Shiga; Yasuhara; Uchiyama; Kondo; Yamanaka
Synthesis, 1992 , # 8 p. 746 - 748
反应条件
sodium carbonate in 1-methyl-pyrrolidin-2-one
参考文献
Roche Vitamins Inc.
Patent: US6573269 B1, 2003 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; hexane T=50°C; 3 h;
参考文献
Sakamoto; Shiga; Yasuhara; Uchiyama; Kondo; Yamanaka
Synthesis, 1992 , # 8 p. 746 - 748
反应条件
T=500°C; P=0.1 - 1 Torr;
参考文献
Aitken, R. Alan; Horsburg, Caroline E. R.; McCreadie, J. Graeme; Seth, Shirley
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1727 - 1732
反应条件
potassium tert-butylate; sodium amide in tetrahydrofuran T=20°C; 2 h;
参考文献
Kim, Joong-Gon; Dong, Ho Kang; Doo, Ok Jang
Synlett, 2008 , # 3 p. 443 - 447
反应条件
1: Et3N / (PPh3)2PdCl2, CuI / 1 h / Ambient temperature 2: p-toluenesulfonic acid / benzene / 12 h / Ambient temperature View Scheme
参考文献
Sakamoto; Shiga; Yasuhara; Uchiyama; Kondo; Yamanaka
Synthesis, 1992 , # 8 p. 746 - 748
反应条件
potassium carbonate in methanol T=60°C; 4 h;
参考文献
Chenault, Jaques; Dupin, Jean-Francois E.
Synthesis, 1987 , # 5 p. 498 - 499
反应条件
ethanol; sodium ethanolate; benzene
参考文献
Butt, G.; Topsom, R. D.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1982 , vol. 38, # 6 p. 649 - 654
反应条件
acetic acid; sodium nitrite in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Beccalli, Egle M.; Manfredi, Amedea; Marchesini, Alessandro
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2372 - 2375
