in neat (no solvent) slight excess over the stoich. amt. of COF2 required; reaction mixt. heated in a stainless steel or monel cylinder at 100°C for 24 h;
参考文献
Mallela, S. P.; Gupta, O. D.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1988 , vol. 27, p. 208 - 209
in neat (no solvent) slight excess over the stoich. amt. of COF2 required; reaction mixt. heated in a stainless steel or monel cylinder at 160°C for 36 h;
参考文献
Mallela, S. P.; Gupta, O. D.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1988 , vol. 27, p. 208 - 209