in neat (no solvent) slight excess over the stoich. amt. of COF2 required; reaction mixt. heated in a stainless steel or monel cylinder at 180°C for 24 h; total yield ca. 65percent;
参考文献
Mallela, S. P.; Gupta, O. D.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1988 , vol. 27, p. 208 - 209
in gas heating the gaseous mixture to 300-700°C through a charcoal containing Pt or C tube;
参考文献
Haszeldine, R. N.; Iserson, H.
Journal of the American Chemical Society, 1957 , vol. 79, p. 5801 - 5804
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Gmelin Handbook: C: MVol.D3, 2.2.8.6.5, page 96 - 97
