1,4-二溴-2,5-双(溴甲基)苯合成路线 （共 4 条）
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane Heating;
参考文献
Lopez-Romero, J. Manuel; Rico, Rodrigo; Martinez-Mallorquin, Rocio; Hierrezuelo, Jesus; Guillen, Elena; Cai, Chengzhi; Otero, J. Carlos; Lopez-Tocon, Isabel
Tetrahedron Letters, 2007 , vol. 48, # 35 p. 6075 - 6079
反应条件
1: 67 percent / Br2; I2 / 16 h / 20 °C 2: 44 percent / N-bromosuccinimide; 1,1'-azobis(cyclohexanecarbonitrile) / benzene / 8 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 21 p. 8522 - 8526
反应条件
1.1: triphenylphosphine / dimethylformamide / 18 h / Heating 1.2: 90 percent / potassium tert-butoxide / tetrahydrofuran 2.1: 94 percent / tetrakis(triphenylphosphine)palladium(0); sodium carbonate / 1,2-dimethoxy-ethane; ethanol; H2O / 16 h / Heating 3.1: 83 percent / bis(tricyclohexylphosphine)(benzylidene)ruthenium dichloride / CH2Cl2 / 23 h / 35 °C View Scheme
参考文献
Bonifacio, Margel C.; Robertson, Charles R.; Jung, Jun-Young; King, Benjamin T.
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8522 - 8526
反应条件
1: AcOH
2: aq. NaOH / ethanol
View Scheme
参考文献
Fan, Qu-Li; Lu, Su; Lai, Yee-Hing; Hou, Xiao-Yuan; Huang, Wei
Macromolecules, 2003 , vol. 36, # 19 p. 6976 - 6984
