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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
353497-31-1
合成路线
（共 9 条）
353497-35-5
→
反应条件
353497-31-1
反应条件
polyphosphoric acid T=90 - 95°C; 3 h;
参考文献
Fuenfschilling, Peter C.; Zaugg, Werner; Beutler, Ulrich; Kaufmann, Daniel; Lohse, Olivier; Mutz, Jean-Paul; Onken, Ulrich; Reber, Jean-Louis; Shenton, David
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 272 - 277
353497-35-5
→
反应条件
3335-98-6
N-苯基吲哚酮
+
353497-31-1
反应条件
PPA T=95°C; 3 h;
参考文献
Kaufmann, Daniel; Fuenfschilling, Peter C.; Beutler, Ulrich; Hoehn, Pascale; Lohse, Olivier; Zaugg, Werner
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5275 - 5278
39507-06-7
→
反应条件
353497-31-1
反应条件
1.1: pyridine / toluene / 24 h / 50 °C 1.2: pyridine / 22 h / 100 °C 2.1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 3.1: 70 percent / polyphosphoric acid / 3 h / 95 °C View Scheme
参考文献
Fuenfschilling, Peter C.; Zaugg, Werner; Beutler, Ulrich; Kaufmann, Daniel; Lohse, Olivier; Mutz, Jean-Paul; Onken, Ulrich; Reber, Jean-Louis; Shenton, David
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 272 - 277
805236-74-2
→
反应条件
353497-31-1
反应条件
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: 70 percent / polyphosphoric acid / 3 h / 95 °C View Scheme
参考文献
Fuenfschilling, Peter C.; Zaugg, Werner; Beutler, Ulrich; Kaufmann, Daniel; Lohse, Olivier; Mutz, Jean-Paul; Onken, Ulrich; Reber, Jean-Louis; Shenton, David
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 272 - 277
3335-98-6
N-苯基吲哚酮
→
反应条件
353497-31-1
反应条件
1.1: sodium hydroxide / tetrahydrofuran / 5 h / 67 °C 1.2: 2 h / -10 °C 2.1: polyphosphoric acid / 3 h / 90 - 95 °C View Scheme
参考文献
Fuenfschilling, Peter C.; Zaugg, Werner; Beutler, Ulrich; Kaufmann, Daniel; Lohse, Olivier; Mutz, Jean-Paul; Onken, Ulrich; Reber, Jean-Louis; Shenton, David
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 272 - 277
353497-31-1
→
反应条件
28721-09-7
10-甲氧卡马西平
反应条件
1: 81 percent / p-TsOH / methanol / 5 h / Heating 2: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C 3: AcOH / 7 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 27 p. 5275 - 5278
353497-31-1
→
反应条件
28721-07-5
奥卡西平
反应条件
1: 81 percent / p-TsOH / methanol / 5 h / Heating 2: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C 3: AcOH / 7 h / 25 °C 4: H2SO4 / 17 h / 25 °C View Scheme
参考文献
Fuenfschilling, Peter C.; Zaugg, Werner; Beutler, Ulrich; Kaufmann, Daniel; Lohse, Olivier; Mutz, Jean-Paul; Onken, Ulrich; Reber, Jean-Louis; Shenton, David
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 272 - 277
353497-31-1
→
反应条件
4698-11-7
10-甲氧基亚氨基芪
反应条件
1: 81 percent / p-TsOH / methanol / 5 h / Heating 2: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 27 p. 5275 - 5278
353497-31-1
→
反应条件
21737-58-6
10,11-二氢-5H-二苯并[b,f]氮杂革-10-酮
反应条件
potassium hydroxide in ethylene glycol T=108°C; 0.5 h;
参考文献
Kaufmann, Daniel; Fuenfschilling, Peter C.; Beutler, Ulrich; Hoehn, Pascale; Lohse, Olivier; Zaugg, Werner
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5275 - 5278
