反应条件
1: Na / 1) NH3(l); 2) DMF, 1 h
2: n-BuLi / 1) diglyme, 80-90 deg C, 6 h; 2) 130-140 deg C, 60 h
3: H2 / Lindlar / ethanol / Ambient temperature
4: m-chloroperoxybenzoic acid / CH2Cl2 / 0 °C
View Scheme
参考文献
Jonas, Jaroslav; Slanina, Pavel; Humpa, Otakar; Mazal, Ctibor
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 4 p. 857 - 859
