2-(4-溴苯氧基)乙酰胺合成路线 (共 3 条)
反应条件
ammonia in methanol T=10 - 30°C; 2.5 h;
参考文献
R-tech Ueno, Ltd.
Patent: WO2009/145360 A1, 2009 ;
Location in patent: Page/Page column 67 ;
WO 2009/145360 A1
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=20°C; 2 h;
参考文献
PFIZER INC.; Bhattacharya, Samit; Cameron, Kimberly; Dowling, Matthew; Fernando, Dilinie; Ebner, David; Filipski, Kevin; Kung, Daniel; Lee, Esther; Smith, Aaron; Tu, Meihua
Patent: US2013/267493 A1, 2013 ;
Location in patent: Paragraph 1027 ;
反应条件
1: sodium ethylate solution 2: alcohol; ammonia View Scheme
参考文献
Powell; Adams
Journal of the American Chemical Society, 1920 , vol. 42, p. 655