1-氧杂环十五烷-2-酮合成路线 （共 40 条）
反应条件
p-NO2-benzoic anhydride; scandium tris(trifluoromethanesulfonate) in tetrahydrofuran; acetonitrile 5 h; Heating; Yields of byproduct given;
参考文献
Ishihara, Kazuaki; Kubota, Manabu; Kurihara, Hideki; Yamamoto, Hisashi
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4560 - 4567
反应条件
4-(N,N-dimethlyamino)pyridine; (2,6-Me(NO2)PhCO)2O in dichloromethane T=20°C; 15 h;
参考文献
Shiina, Isamu; Kubota, Mari; Oshiumi, Hiromi; Hashizume, Minako
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1822 - 1830
反应条件
tetraoctylammonium (2-pyrrolidonide) in N,N-dimethyl-formamide 24 h; Ambient temperature;
参考文献
Shono, Tatsuya; Ishige, Osamu; Uyama, Hiroshi; Kashimura, Shigenori
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 546 - 549
反应条件
caesium carbonate in N,N-dimethyl-formamide T=40°C; Title compound not separated from byproducts;
参考文献
Kruizinga, Wim H.; Kellogg, Richard M.
Journal of the American Chemical Society, 1981 , vol. 103, # 17 p. 5183 - 5189
反应条件
hydrogenchloride; zinc in diethyl ether T=-10°C; 7 h;
参考文献
Kostova, Kalina; Hesse, Manfred
Helvetica Chimica Acta, 1995 , vol. 78, # 2 p. 440 - 446
反应条件
potassium peroxomonosulphate; sulfuric acid; Petroleum ether T=43 - 44°C;
参考文献
Kruizinga, Wim H.; Kellogg, Richard M.
Journal of the American Chemical Society, 1981 , vol. 103, # 17 p. 5183 - 5189
反应条件
1: 47percent HBr / toluene / Heating 2: NaI / acetone / Ambient temperature 3: p-TolSO3H / benzene / Heating 4: 86 percent / NaBH3CN / methanol / 3 h / Ambient temperature; Irradiation View Scheme
参考文献
Porter,N.A.; Chang,V.H.T.
Journal of the American Chemical Society, 1987 , vol. 109, p. 4976
反应条件
1: NaI / acetone / Ambient temperature 2: p-TolSO3H / benzene / Heating 3: 86 percent / NaBH3CN / methanol / 3 h / Ambient temperature; Irradiation View Scheme
参考文献
Porter,N.A.; Chang,V.H.T.
Journal of the American Chemical Society, 1987 , vol. 109, p. 4976
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=110°C; 1 h;
参考文献
Kostova, Kalina; Hesse, Manfred
Helvetica Chimica Acta, 1995 , vol. 78, # 2 p. 440 - 446
反应条件
1: sodium iodide / butan-2-one / 3 h / Heating 2: 45 percent / tertbutyltin hydride, AIBN / benzene / 3 h / Heating View Scheme
参考文献
Porter,N.A.; Chang,V.H.T.
Journal of the American Chemical Society, 1987 , vol. 109, p. 4976
