2-(3-氯苯氧基)硫代乙酰胺合成路线 （共 6 条）
反应条件
tetraphosphorus decasulfide in tetrahydrofuran T=50°C; 1.5 h;
参考文献
Li, Ting; Liu, Guyue; Li, Hongcai; Yang, Xinmei; Jing, Yongkui; Zhao, Guisen
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2316 - 2322
反应条件
1: sodium hydroxide / 100 °C 2: thionyl chloride / 4 h / 80 °C 3: ammonia / water; toluene / 1.5 h / 0 - 5 °C 4: tetraphosphorus decasulfide / tetrahydrofuran / 1.5 h / 50 °C View Scheme
参考文献
Li, Ting; Liu, Guyue; Li, Hongcai; Yang, Xinmei; Jing, Yongkui; Zhao, Guisen
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2316 - 2322
反应条件
1: ammonia / water; toluene / 1.5 h / 0 - 5 °C 2: tetraphosphorus decasulfide / tetrahydrofuran / 1.5 h / 50 °C View Scheme
参考文献
Li, Ting; Liu, Guyue; Li, Hongcai; Yang, Xinmei; Jing, Yongkui; Zhao, Guisen
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2316 - 2322
反应条件
1: thionyl chloride / 4 h / 80 °C 2: ammonia / water; toluene / 1.5 h / 0 - 5 °C 3: tetraphosphorus decasulfide / tetrahydrofuran / 1.5 h / 50 °C View Scheme
参考文献
Li, Ting; Liu, Guyue; Li, Hongcai; Yang, Xinmei; Jing, Yongkui; Zhao, Guisen
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2316 - 2322
参考文献
Djerassi; Scholz
Journal of Organic Chemistry, 1950 , vol. 15, p. 694,695, 698
反应条件
(i) aq. NH3, (ii) P2S5, benzene; Multistep reaction;
参考文献
Abdel-Lateef,M.F.-A.; Eckstein,Z.
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1971 , vol. 19, # 11-12 p. 705 - 711
