4-碘-3-甲氧基苯甲酸甲酯合成路线 (共 21 条)
反应条件
1: sodium hydroxide; sodium iodide; sodium hypochlorite / methanol / 2 h / -10 - 3 °C 2: sulfuric acid / |Reflux 3: potassium carbonate / acetone / 4 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Chemical Communications (Cambridge, United Kingdom), , vol. 48, # 83 p. 10328 - 10330,3
反应条件
1: ICl, aq. HCl 2: KMnO4 View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 15, p. 1174 - 1177
反应条件
1: KMnO4 View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 15, p. 1174 - 1177
反应条件
1: aq. Ba(OH)2 2: ICl, aq. HCl 3: KMnO4 View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 15, p. 1174 - 1177
反应条件
1: 82 percent / HCl / Heating 2: 86 percent / NaNO2; KI; HCl / 0 °C 3: 100 percent / NaH / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 9 p. 1269 - 1273
反应条件
1: 86 percent / NaNO2; KI; HCl / 0 °C 2: 100 percent / NaH / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 9 p. 1269 - 1273
参考文献
Journal of Medicinal Chemistry, , vol. 15, p. 1174 - 1177
参考文献
Chemische Berichte, , vol. 56, p. 847
反应条件
1: 97 percent / Et3N, Pd(OAc)2, P(o-Tol)3 / dimethylformamide / 3 h / 100 °C 2: KOH / ethanol / 3 h / Heating View Scheme
参考文献
European Journal of Inorganic Chemistry, , # 5 p. 613 - 619
反应条件
1: With bis[2-(N,N-dimethylamino)ethyl] ether; isopropylmagnesium chloride in tetrahydrofuran
2: With boric acid trimethyl ester in tetrahydrofuran
参考文献
Wang, Xiao-Jun; Sun, Xiufeng; Zhang, Li; Xu, Yibo; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Organic Letters, 2006 , vol. 8, # 2 p. 305 - 307