3-碘-4-甲氧基苯甲酸甲酯合成路线 （共 16 条）
反应条件
indium trifluoromethanesulfonate; N-iodo-succinimide in acetonitrile T=23°C; 36 h; Inert atmosphereDarkness;
参考文献
Organic Letters, , vol. 12, # 9 p. 2104 - 2107
反应条件
sodium hydrogen telluride; acetic acid in ethanol 4 h; Heating; Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 3911 - 3917
反应条件
1: 64 percent / MeONa / dimethylformamide / Ambient temperature 2: Na2Se, NaBH4 / 4 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 3911 - 3917
反应条件
potassium carbonate in acetone
参考文献
Synlett, , # 13 p. 2005 - 2008
反应条件
sodium selenide; sodium tetrahydroborate 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 3911 - 3917
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 59, p. 143
反应条件
1: copper-powder / 260 °C 2: aqueous hydriodic acid 3: concentrated aqueous HCl / 270 °C View Scheme
参考文献
Sugii
Yakugaku Zasshi, 1930 , vol. 50, p. 183,201; dtsch. Ref. S. 24
Chem.Abstr., 1930 , p. 3505
反应条件
TlOH; tetrakis(triphenylphosphine) palladium(0) in benzene Dehalogenation; Suzuki cross-coupling; Heating;
参考文献
Tetrahedron, , vol. 56, # 49 p. 9655 - 9662
反应条件
Ti2CO3; tetrakis(triphenylphosphine) palladium(0) in benzene Suzuki cross-coupling; 168 h; Heating;
参考文献
Chaumeil; Signorella; Le Drian
Tetrahedron, 2000 , vol. 56, # 49 p. 9655 - 9662
反应条件
aluminium trichloride in dichloromethane; ethanethiol 6.5 h; temp. 0 deg C -> RT;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 31, # 2 p. 749 - 751
