反应条件
in further solvent(s) soln. of CF2=CHBF2 in 1,1,1,3,3-pentafluoropropane and 1,1,1,3,3-pentafluorobutane cooled to -60°C and XeF2 added in one portion; stirredat -60 to -62°C for 2 h and left for 15 min without stirring; decanted; precipitate treated in vacuum at -60°C; unknown byproducts detected by NMR;
参考文献
Frohn, Hermann-Josef; Bardin, Vadim V.
Zeitschrift fur Anorganische und Allgemeine Chemie, 2003 , vol. 629, # 14 p. 2465 - 2469