in monofluoro-trichloromethane 24 h; -141 degC to 25 degC; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 64, # 1-2 p. 129 - 150
in monofluoro-trichloromethane 20 h; -140 degC to 22 degC; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 64, # 1-2 p. 129 - 150
Eleev, A. F.; Vasil'ev, N. V.; Sokol'skii, G. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # l p. 250 - 255
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 2 p. 280 - 286
in further solvent(s) solvent: Genetron 113, excess of WF6, at -80°C, allowed to warm slowly to room temp., gently warmed for 15 min to about 30°C, left to stand at room temp. for 2 h; solvent and excess WF6 distilled, warmed to 45°C under dynamic vacuum, recrystn. (trifluoroacetic acid);
