2,2,2-三氟乙酰胺合成路线 (共 158 条)
反应条件
hydrogenchloride; triethylamine in ethanol; ethyl acetate
参考文献
PE Corporation (NY)
Patent: US6448407 B1, 2002 ;
反应条件
triethylamine in Pestox XIV; dichloromethane
反应条件
zirconium tetrachloride; ammonium carbamate in toluene T=120°C; 24 h; Inert atmosphereMolecular sieve;
参考文献
Tinnis, Fredrik; Lundberg, Helena; Adolfsson, Hans
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2531 - 2536
反应条件
acetyl chloride in chloroform T=20°C; 3 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 2314 - 2315
Zhurnal Organicheskoi Khimii, , vol. 19, # 12 p. 2632 - 2633
反应条件
potassium meta-periodate; [{Ru(η3:η3-C10H16)(μ-Cl)Cl}2] in water T=100°C; 1 h;
参考文献
Cadierno, Victorio; Gimeno, Jose; Nebra, Noel
Chemistry - A European Journal, 2007 , vol. 13, # 23 p. 6590 - 6594
反应条件
in neat (no solvent) T=230°C; 0.333333 h;
参考文献
Tanaka, Chiaki; Nasu, Keiko; Yamamoto, Noriko; Shibata, Megumi
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 9 p. 3374 - 3376
反应条件
in trifluoroacetic acid T=230°C; 0.333333 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 9 p. 3374 - 3376
反应条件
in neat (no solvent) T=230°C; 0.5 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 9 p. 3374 - 3376
反应条件
cyclohexene in dichloromethane T=15 - 20°C; 0.2 h; Irradiation; Yields of byproduct given;
参考文献
Lessard, Jean; Mondon, Martine; Touchard, Daniel
Canadian Journal of Chemistry, 1981 , vol. 59, p. 431 - 450