2,2,2-三氟乙酰胺合成路线 （共 158 条）
反应条件
trifluoroacetic acid; silver(l) oxide anschliessendes Behandeln mit Brom;
参考文献
Beebe,T.R.; Wolfe,J.W.
Journal of Organic Chemistry, 1970 , vol. 35, p. 2056 - 2057
反应条件
3 A molecular sieve; potassium carbonate; tris-(dibenzylideneacetone)dipalladium(0) in tert-butyl alcohol T=110°C; 24 h;
参考文献
Ikawa, Takashi; Barder, Timothy E.; Biscoe, Mark R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2007 , vol. 129, # 43 p. 13001 - 13007
反应条件
potassium carbonate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in 1,4-dioxane T=75°C;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in N,N-dimethyl-formamide T=45°C;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
potassium carbonate; tetrabutylammomium bromide in acetonitrile T=80°C; 2 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
反应条件
potassium carbonate; tetrabutylammomium bromide in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
反应条件
in tetrachloromethane after addition heating to 70°C (6 h);
参考文献
Arbuzov, B. A.; Zobova, N. N.; Andronova, I. I.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1974 , p. 1484 - 1487
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1974 , p. 1566 - 1570
C.A., 1974 , vol. 81, p. 169072
参考文献
Ye; Noftle
Journal of Fluorine Chemistry, 1997 , vol. 81, # 2 p. 193 - 196
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in N,N-dimethyl-formamide T=45°C;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
In alcaline soln. at 0°C.;
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
