2,2,2-三氟乙酰胺合成路线 （共 158 条）
参考文献
Gayral; Bourdais; Lorre; et al.
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 2 p. 171 - 175
反应条件
1: methyllithium With cerium(III) chloride in diethyl ether
T=-78°C; 0.5 h;
2: trifluoromethyl amino ketone in tetrahydrofuran; diethyl ether
T=-78 - 20°C;
参考文献
Zhang, Nan; Ayral-Kaloustian, Semiramis
Journal of Fluorine Chemistry, 2002 , vol. 117, # 1 p. 9 - 11
反应条件
NaF
byproducts: HF; 20°C, 48 h;
参考文献
Stahl, I.; Mews, R.; Glemser, O.
Z. Naturforsch. b, 1978 , vol. 33, p. 1417 - 1421
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.2, page 1 - 48
反应条件
in solid
other Radiation; electron radiation of CF3CONH2;; determination by ESR;;
参考文献
Rogers; Kispert
Journal of Chemical Physics, 1967 , vol. 46, p. 3193
反应条件
potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride in acetonitrile
T=25°C; 48 h;
参考文献
Landini, Dario; Penso, Michele
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 420 - 423
反应条件
in further solvent(s)
addition of AgF suspension at 50-60°C then 0.5 h reflux in fluorohydrocarbon;
参考文献
Young,J.A. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 4553 - 4556
参考文献
Young,J.A. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 4553 - 4556
参考文献
Nishikawa, Shiro; Nishikimi, Yoshio; Maki, Shinji; Kumazawa, Zenzaburo; Kashimura, Naoki
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 4 p. 1034 - 1038
参考文献
Gayral; Bourdais; Lorre; et al.
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 2 p. 171 - 175
反应条件
trichlorophosphate in toluene
4 h; Heating;
参考文献
Arbuzov, B. A.; Aganov, A. V.; Zobova, N. N.; Klochkov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 4 p. 544 - 548
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 4 p. 758 - 762
