2,2,2-三氟乙酰胺合成路线 (共 158 条)
反应条件
in chloroform T=20°C; 1440 h; Mechanism;
参考文献
Chkanikov, N. D.; Vershinin, V. L.; Galakhov, M. V.; Kolomiets, A. F.; Fokin, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 1.2 p. 113 - 119
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 38, # 1 p. 126 - 132
参考文献
Journal of chromatography, , vol. 78, # 2 p. 273 - 279
F: PerFHalOrg.7, 1, page 1 - 84
参考文献
Journal of chromatography, , vol. 78, # 2 p. 273 - 279
F: PerFHalOrg.7, 1, page 1 - 84
参考文献
Journal of chromatography, , vol. 78, # 2 p. 273 - 279
F: PerFHalOrg.7, 1, page 1 - 84
参考文献
Journal of Fluorine Chemistry, , vol. 81, # 2 p. 193 - 196
反应条件
potassium carbonate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in 1,4-dioxane T=75°C;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in N,N-dimethyl-formamide T=45°C;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium hydrogencarbonate in 1,4-dioxane T=90°C; Addition; ring cleavage;
参考文献
Tetrahedron, , vol. 53, # 13 p. 4787 - 4790
反应条件
potassium carbonate in water T=20°C; 2 h;
参考文献
Hartung, Rainer; Golz, Gregor; Schlaf, Susanne; Silvennoinen, Gudrun; Polborn, Kurt; Mayer, Peter; Pfaendler, Hans Rudolf
Synthesis, 2009 , # 3 p. 495 - 501
反应条件
sodium hydride 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Harland, Philip A.; Hodge, Philip; Maughan, Wilfrid; Wildsmith, Eric
Synthesis, 1984 , # 11 p. 941 - 943