2,2,2-三氟乙酰胺合成路线 （共 158 条）
参考文献
American Home Products Corporation
Patent: US5187168 A1, 1993 ;
反应条件
-40°C, then 50-60°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
参考文献
Minnesota Mining and Mfg.Co.
Patent: US2701814 , 1953 ;
反应条件
potassium carbonate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in 1,4-dioxane T=75°C; 24 h;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in N,N-dimethyl-formamide T=45°C; 24 h;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
Lawesson's reagent in tetrahydrofuran 2 h; Heating / reflux;
参考文献
Dow AgroSciences LLC
Patent: US6372769 B1, 2002 ;
Location in patent: Page column 3 ;
参考文献
ROHM AND HAAS COMPANY
Patent: EP1110454 A2, 2001 ;
Title/Abstract Full Text Show Details
ROHM AND HAAS COMPANY
Patent: EP1108714 A1, 2001 ;
反应条件
potassium carbonate; tetrabutylammomium bromide in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
反应条件
potassium carbonate; tetrabutylammomium bromide in N,N-dimethyl-formamide T=50°C; 24 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
反应条件
potassium carbonate; tetrabutylammomium bromide in N,N-dimethyl-formamide T=80°C; 6 h;
参考文献
Landini, Dario; Penso, Michele
Synthetic Communications, 1988 , vol. 18, # 8 p. 791 - 800
